anthracene-1,2-diyl diacetate

Base Information

• Chemical Name: anthracene-1,2-diyl diacetate
• CAS No.: 74877-26-2
• Molecular Formula: C18H14O4
• Molecular Weight: 294.307
• Mol file: 74877-26-2.mol

Synonyms:

Chemical Property of anthracene-1,2-diyl diacetate

Chemical Property:

• Vapor Pressure: 2.67E-09mmHg at 25°C
• Boiling Point: 478°C at 760 mmHg
• Flash Point: 246.7°C
• Density: 1.263g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of anthracene-1,2-diyl diacetate

There total 6 articles about anthracene-1,2-diyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

1,2-dihydroxyanthracene (577-95-7) + acetic anhydride (108-24-7) → 1,2-diacetoxy-anthracene (74877-26-2)

Guidance literature:

In pyridine;

DOI:10.1021/jo01310a029

Reference yield:

1,2-anthraquinone (655-04-9) → 1,2-diacetoxy-anthracene (74877-26-2)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether

2: 31 percent / pyridine

With lithium aluminium tetrahydride; In pyridine; diethyl ether;

DOI:10.1021/jo01310a029

Reference yield:

2-hydroxyanthracene (613-14-9) → 1,2-diacetoxy-anthracene (74877-26-2)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid / und anschliessend mit wss.HCl

2: aqueous H₂O₂; aqueous NaOH; pyridine

3: sodium acetate

With pyridine; sodium hydroxide; dihydrogen peroxide; sodium acetate; acetic acid;

upstream raw materials:

diacetylalizarin

acetic anhydride

1,2-dihydroxyanthracene

1,2-anthraquinone

Downstream raw materials:

trans-1,2-dihydroxy-1,2-dihydroanthracene

diacetylalizarin

1,2-dihydroxy-9,10-anthracenedione

Refernces