Dicycloocta[b,e][1,4]dithiin,1,2,3,4,5,6,8,9,10,11,- 12,13-dodecahydro-

Base Information

• Chemical Name: Dicycloocta[b,e][1,4]dithiin,1,2,3,4,5,6,8,9,10,11,- 12,13-dodecahydro-
• CAS No.: 4427-65-0
• Molecular Formula: C₁₆H₂₄S₂
• Molecular Weight: 280.499
• Mol file: 4427-65-0.mol

Synonyms:

Chemical Property of Dicycloocta[b,e][1,4]dithiin,1,2,3,4,5,6,8,9,10,11,- 12,13-dodecahydro-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dicycloocta[b,e][1,4]dithiin,1,2,3,4,5,6,8,9,10,11,- 12,13-dodecahydro-

There total 1 articles about Dicycloocta[b,e][1,4]dithiin,1,2,3,4,5,6,8,9,10,11,- 12,13-dodecahydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclooctyne (1781-78-8) + 9-Thiofluorenone S-oxide (4440-32-8) → 1,2,3,4,5,6,8,9,10,11,12,13-dodecahydrodicycloocta[1,4]dithiin (4427-65-0) + 9-fluorenone (486-25-9,952573-42-1) + C16H26OS + 2-fluoren-9-ylidene-cyclooctanone

Guidance literature:

In methanol; dichloromethane; at 50 ℃; for 48h; Product distribution; other solvent, temperatures, reaction times, effects of irradiation, reagent ratio, presence of air;

DOI:10.1021/jo9816764

upstream raw materials:

cyclooctyne

9-Thiofluorenone S-oxide

Refernces