Ethylamine, 2-(o-chlorophenoxy)-N-methyl-,

Base Information

• Chemical Name: Ethylamine, 2-(o-chlorophenoxy)-N-methyl-,
• CAS No.: 70289-29-1
• Molecular Formula: C₉H₁₂ClNO
• Molecular Weight: 185.653
• Hs Code.: 2922299090
• Mol file: 70289-29-1.mol

Synonyms:Ethylamine,2-(o-chlorophenoxy)-N-methyl- (6CI,7CI);N-[2-(2-Chlorophenoxy)ethyl]methylamine

Chemical Property of Ethylamine, 2-(o-chlorophenoxy)-N-methyl-,

Chemical Property:

• Vapor Pressure: 0.00668mmHg at 25°C
• Boiling Point: 270.8°C at 760 mmHg
• Flash Point: 117.6°C
• PSA: 21.26000
• Density: 1.11g/cm³
• LogP: 2.32910

Purity/Quality:

[2-(2-chlorophenoxy)ethyl](methyl)amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethylamine, 2-(o-chlorophenoxy)-N-methyl-,

There total 3 articles about Ethylamine, 2-(o-chlorophenoxy)-N-methyl-, which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2-bromoethoxy)-2-chlorobenzene (18800-26-5) + methylamine (74-89-5) → [2-(2-chloro-phenoxy)-ethyl]-methyl-amine (70289-29-1)

Guidance literature:

In methanol; at 100 ℃; for 12h;

DOI:10.1021/jm030944+

Reference yield:

2-monochlorophenol (95-57-8) → [2-(2-chloro-phenoxy)-ethyl]-methyl-amine (70289-29-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH / 7 h / 100 °C

2: methanol / 12 h / 100 °C

With sodium hydroxide; In methanol;

DOI:10.1021/jm030944+

Reference yield:

1-(2-bromoethoxy)-2-chlorobenzene (18800-26-5) → [2-(2-chloro-phenoxy)-ethyl]-methyl-amine (70289-29-1)

Guidance literature:

With ethanol; methylamine;

upstream raw materials:

1-(2-bromoethoxy)-2-chlorobenzene

methylamine

2-monochlorophenol

Downstream raw materials:

[2-(2-Chloro-phenoxy)-ethyl]-{2-[2-(2-{[2-(2-chloro-phenoxy)-ethyl]-methyl-amino}-ethoxy)-ethoxy]-ethyl}-methyl-amine

Refernces