Technology Process of Benzenepropanoic acid, a-nitro-, methyl ester
There total 14 articles about Benzenepropanoic acid, a-nitro-, methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
HOF* CH3CN; sodium fluoride;
In
dichloromethane; water; acetonitrile;
for 0.0833333h;
Ambient temperature;
DOI:10.1021/jo00084a047
- Guidance literature:
-
With
N-benzyl-N,N,N-triethylammonium chloride; potassium hydrogencarbonate;
In
N,N-dimethyl-formamide;
at 60 ℃;
for 16h;
- Guidance literature:
-
methyl 2-nitroacetate; benzaldehyde;
With
titanium tetrachloride;
In
tetrahydrofuran; tetrachloromethane;
at 0 ℃;
for 2h;
With
4-methyl-morpholine;
In
tetrahydrofuran; tetrachloromethane;
at 18 ℃;
for 20h;
With
sodium tetrahydroborate; silica gel;
In
chloroform; isopropyl alcohol;
at 20 ℃;
for 4h;
DOI:10.1021/ja0343151