Technology Process of 5-Benzylcyclohexane-1,3-dione
There total 9 articles about 5-Benzylcyclohexane-1,3-dione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(E)-6-phenyl-3-hexen-2-one; sodium ethanolate;
With
diethyl malonate;
In
ethanol;
at 25 - 60 ℃;
Reflux;
With
sodium hydroxide;
In
ethanol;
at 80 ℃;
for 2h;
With
hydrogenchloride;
In
ethanol; water;
for 1h;
pH=2;
Reflux;
DOI:10.1021/jm401939g
- Guidance literature:
-
5-phenyl-pent-3-en-2-one; diethyl malonate;
With
sodium ethanolate;
In
ethanol;
for 12h;
With
sodium hydroxide;
In
ethanol; water;
for 12h;
With
hydrogenchloride;
In
diethyl ether; water;
DOI:10.1016/j.bmc.2011.11.039
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethylamine; absolute alcohol
2: sodium salt of acetoacetic acid ester; alcohol / Verseifen des Reaktionsprodukts mit Sodaloesung
With
ethanol; sodium aceto-acetate; diethylamine;
