4-iodosylbenzoic Acid

Base Information

• Chemical Name: 4-iodosylbenzoic Acid
• CAS No.: 4230-36-8
• Molecular Formula: C7H5IO3
• Molecular Weight: 264.019
• DSSTox Substance ID: DTXSID10415989
• Nikkaji Number: J337.125E
• Wikidata: Q82225093
• Mol file: 4230-36-8.mol

Synonyms:4-iodosylbenzoic Acid;p-Jodosobenzoesaure;4-Iodosobenzoic acid;4230-36-8;SCHEMBL8461234;DTXSID10415989

Chemical Property of 4-iodosylbenzoic Acid

Chemical Property:

• XLogP3: 2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 263.92834
• Heavy Atom Count: 11
• Complexity: 161

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C(=O)O)I=O

Technology Process of 4-iodosylbenzoic Acid

There total 3 articles about 4-iodosylbenzoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-dichloroiodanyl-benzoic acid (22695-77-8) → 4-iodosyl-benzoic acid (4230-36-8)

Guidance literature:

With phosphate-buffer solution; Hydrolysis;

DOI:10.1021/ja01117a056

Reference yield:

4-iodobenzoic acid (619-58-9) → 4-iodosyl-benzoic acid (4230-36-8)

Guidance literature:

With chlorine; acetic acid; man loest das Jodidchlorid in verd. Natronlauge und saeuert mit verd. Schwefelsaeure an;

Reference yield:

4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) → 4-iodosyl-benzoic acid (4230-36-8)

Guidance literature:

Multi-step reaction with 2 steps

1: diluted sulfuric acid / Diazotization_.Umsetzung der Diazoniumsalzloesung mit KI

2: glacial acetic acid; chlorine / man loest das Jodidchlorid in verd. Natronlauge und saeuert mit verd. Schwefelsaeure an

With sulfuric acid; chlorine; acetic acid;

upstream raw materials:

4-iodobenzoic acid

4-dichloroiodanyl-benzoic acid

4-amino-benzoic acid

Downstream raw materials:

4-iodobenzoic acid

4-iodylbenzoic acid