Carbamodithioic acid, dimethyl-, 1-phenylethyl ester

Base Information

• Chemical Name: Carbamodithioic acid, dimethyl-, 1-phenylethyl ester
• CAS No.: 42600-22-6
• Molecular Formula: C11H15NS2
• Molecular Weight: 225.379
• Mol file: 42600-22-6.mol

Synonyms:

Chemical Property of Carbamodithioic acid, dimethyl-, 1-phenylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Carbamodithioic acid, dimethyl-, 1-phenylethyl ester

There total 2 articles about Carbamodithioic acid, dimethyl-, 1-phenylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

Thiram (137-26-8,93196-73-7) + (1-chloroethyl)benzene (672-65-1) → 1-phenethyl dimethylcarbamodithioate (42600-22-6)

Guidance literature:

With caesium carbonate; In dimethyl sulfoxide; at 20 ℃; for 24h;

DOI:10.1002/ejoc.201801449

Reference yield:

benzyl dimethyldithiocarbamate (7250-18-2) + methyl iodide (74-88-4) → 1-phenethyl dimethylcarbamodithioate (42600-22-6)

Guidance literature:

Multistep reaction; (i) lithiumdiisopropylamide, THF, hexane, (ii) /BRN= 969135/;

DOI:10.1021/ja00839a073

upstream raw materials:

benzyl dimethyldithiocarbamate

methyl iodide

Thiram

(1-chloroethyl)benzene

Refernces