2,2'-Azobisquinoline

Base Information

• Chemical Name: 2,2'-Azobisquinoline
• CAS No.: 4289-26-3
• Molecular Formula: C18H12N4
• Molecular Weight: 0.00000
• Mol file: 4289-26-3.mol

Synonyms:

Chemical Property of 2,2'-Azobisquinoline

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2'-Azobisquinoline

There total 6 articles about 2,2'-Azobisquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

N,N'-di-[2]quinolyl-hydrazine (100146-17-6) → 1,2-bis(quinolin-2-yl)diazene (4289-26-3)

Guidance literature:

With iron(III) chloride; In water; acetone; Heating;

DOI:10.1080/00397919908085972

Reference yield: 54.0%

N-(quinolin-2-yl)pyridinium aminide (157020-15-0) → 1,2-bis(quinolin-2-yl)diazene (4289-26-3)

Guidance literature:

With N-chloro-succinimide; In dichloromethane; at 20 ℃;

DOI:10.1016/j.tet.2018.03.064

Reference yield:

2-Chloroquinoline (612-62-4) → [2,2']Azochinolin (6425-85-0,4289-26-3)

Guidance literature:

With hydrazine hydrate; at 140 ℃; Behandeln des Reaktionsprodukts in wss. Essigsaeure mit nitrosen Gasen;

DOI:10.1039/jr9550002816

upstream raw materials:

2-Chloroquinoline

N,N'-di-[2]quinolyl-hydrazine

N-(quinolin-2-yl)pyridinium aminide

Downstream raw materials:

N,N'-di-[2]quinolyl-N-phenyl hydrazine

Refernces

• 1、 Wang, Cai-Lan,Wang, Xiao-Xia,Wang, Xiao-Yang,Xiao, Jun-Ping,Wang, Yu-Lu. "A convenient method for dehydrogenation of symmetric hydrazo compounds". . p. 3435 - 3438. Retrieved 2007/10/03.
• 2、 -. "Evaporator system comprising a stabilized pesticidal phosphoric acid ester and method for stabilizing such ester enclosed in an evaporator". . . Retrieved 2008/06/13.