Ethanediamide, N,N'-dipropyl-

Base Information

• Chemical Name: Ethanediamide, N,N'-dipropyl-
• CAS No.: 14040-77-8
• Molecular Formula: C8H16N2O2
• Molecular Weight: 172.227
• Hs Code.: 2924199090
• European Community (EC) Number: 668-511-7
• DSSTox Substance ID: DTXSID10930783
• Nikkaji Number: J752.951A
• Wikidata: Q82906206
• Mol file: 14040-77-8.mol

Synonyms:Ethanediamide, N,N'-dipropyl-;N,N'-dipropyloxamide;N1,N2-dipropylethanediamide;14040-77-8;N,N'-Dipropylethanediamide;N,N'-Dipropyl-oxalamide;N1,N2-Dipropyloxalamide;N,N-Dipropylethanediamide;SCHEMBL6858080;DTXSID10930783;N~1~,N~2~-Dipropylethanediamide;MFCD00027894;STK868759;AKOS003251756;Oxalic acid, diamide, N,N'-dipropyl-;CS-0328779;A1-01274

Chemical Property of Ethanediamide, N,N'-dipropyl-

Chemical Property:

• PSA: 58.20000
• Density: 0.998 g/cm³
• LogP: 0.82060
• XLogP3: 1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 172.121177757
• Heavy Atom Count: 12
• Complexity: 139

Purity/Quality:

99% ^*data from raw suppliers

N,N'-Dipropyl-oxalamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCCNC(=O)C(=O)NCCC

Technology Process of Ethanediamide, N,N'-dipropyl-

There total 11 articles about Ethanediamide, N,N'-dipropyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

propylamine (107-10-8,42939-71-9) + oxalic acid diethyl ester (95-92-1) → N,N'-dipropyloxamide (14040-77-8)

Guidance literature:

With lithium bromide; at 20 ℃;

DOI:10.1007/s00706-010-0325-1

Reference yield: 90.0%

propylamine (107-10-8,42939-71-9) + oxalyl dichloride (79-37-8) → N,N'-dipropyloxamide (14040-77-8)

Guidance literature:

at -17 ℃; for 2h;

DOI:10.1021/jf9601426

Reference yield: 81.0%

propylamine (107-10-8,42939-71-9) + diisopropenyl oxalate (148705-17-3) → N,N'-dipropyloxamide (14040-77-8)

Guidance literature:

In ethyl acetate; for 0.5h; Ambient temperature;

DOI:10.1016/S0040-4020(01)86342-0

upstream raw materials:

propylamine

oxalic acid diethyl ester

1,6-Dihydroxy-2,5-dicyan-hexatrien-(1,3^trans,5)-dicarbonsaeure-(1,6)-diaethylester

carbon monoxide

Refernces

• 1、 Larisch, Bernd,Pischetsrieder, Monika,Severin, Theodor. "Reactions of dehydroascorbic acid with primary aliphatic amines including Nα-acetyllysine". . p. 1630 - 1634. Retrieved 1996.
• 2、 Abaee, M. Saeed,Akbarzadeh, Elahe,Sharifi, Roholah,Mojtahedi, Mohammad M.. "Environmentally friendly transesterification and transacylation reactions under libr catalysis". experimental part. p. 757 - 761. Retrieved 2011/07/08.