Iodonium,(4-methoxyphenyl)(4-nitrophenyl)-, bromide (1:1)

Base Information

• Chemical Name: Iodonium,(4-methoxyphenyl)(4-nitrophenyl)-, bromide (1:1)
• CAS No.: 4072-45-1
• Molecular Formula: Br*C₁₃H₁₁INO₃
• Molecular Weight: 436.044
• Mol file: 4072-45-1.mol

Synonyms:(p-Methoxyphenyl)(p-nitrophenyl)iodoniumbromide (7CI); Iodonium, (4-methoxyphenyl)(4-nitrophenyl)-, bromide (9CI);Iodonium, (p-methoxyphenyl)(p-nitrophenyl)-, bromide (8CI); NSC 86356

Chemical Property of Iodonium,(4-methoxyphenyl)(4-nitrophenyl)-, bromide (1:1)

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Iodonium,(4-methoxyphenyl)(4-nitrophenyl)-, bromide (1:1)

There total 1 articles about Iodonium,(4-methoxyphenyl)(4-nitrophenyl)-, bromide (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-nitrobenzene iodide (636-98-6) + methoxybenzene (100-66-3) → 4-methoxy-4'-nitrodiphenyliodonium bromide (4072-45-1)

Guidance literature:

Multistep reaction; (i) K₂S₂O₈, H₂SO₄, (ii) /BRN= 506892/, (iii) aq. NaBr;

DOI:10.1021/jm00320a017

upstream raw materials:

p-nitrobenzene iodide

methoxybenzene

Refernces

• 1、 Kazmierczak,Skulski. "A short-cut synthesis of diaryliodonium bromides followed by oxidative anion metatheses". . p. 1027 - 1032. Retrieved 2007/10/02.