1,3,6,8-Pyrenetetrasulfonic acid, tetrasodium salt

Base Information

• Chemical Name: 1,3,6,8-Pyrenetetrasulfonic acid, tetrasodium salt
• CAS No.: 59572-10-0
• Deprecated CAS: 1313437-48-7
• Molecular Formula: C16H10 O12 S4 . 4 Na
• Molecular Weight: 610.44
• Hs Code.: 29049090
• European Community (EC) Number: 626-424-1
• UNII: P062LD4V71
• DSSTox Substance ID: DTXSID9041233
• Nikkaji Number: J429.391F
• Wikidata: Q27285958
• Mol file: 59572-10-0.mol

Synonyms:59572-10-0;1,3,6,8-pyrenetetrasulfonic acid tetrasodium salt;Sodium pyrene-1,3,6,8-tetrasulfonate;1,3,6,8-Pyrenetetrasulfonic acid, tetrasodium salt;Tetrasodium 1,3,6,8-pyrenetetrasulfonate;Trasar 23299;tetrasodium;pyrene-1,3,6,8-tetrasulfonate;DTXSID9041233;P062LD4V71;MFCD00042029;1,3,6,8-Pyrenetetrasulfonic acid, sodium salt (1:4);pyrene-1,3,6,8-tetrasulfonic acid tetrasodium salt;UNII-P062LD4V71;C16H6Na4O12S4;PERFLUOROOCTANOYLFLUORIDE;Pyrene-1,3,6,8-tetrasulfonic acid tetra sodium salt;DTXCID7021233;Tox21_303858;Sodiumpyrene-1,3,6,8-tetrasulfonate;AKOS027378630;NCGC00357123-01;SY076372;CAS-59572-10-0;FT-0606535;Tetrasodium pyrene-1,3,6,8-tetrasulphonate;D83387;1,3,6,8-TETRASODIUM PYRENETETRASULFONATE;Q27285958

Chemical Property of 1,3,6,8-Pyrenetetrasulfonic acid, tetrasodium salt

Chemical Property:

• Appearance/Colour: green fine crystalline powder
• Vapor Pressure: 0Pa at 25℃
• Melting Point: 102-104°C(lit.)
• Boiling Point: 337-466℃
• PSA: 262.32000
• Density: 2.015-2.15
• LogP: 4.52360
• Storage Temp.: Inert atmosphere,Room Temperature
• Solubility.: Soluble in water
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 12
• Rotatable Bond Count: 0
• Exact Mass: 609.8332874
• Heavy Atom Count: 36
• Complexity: 942

Purity/Quality:

99.9% ^*data from raw suppliers

1,3,6,8-PyrenetetrasulfonicAcidTetrasodiumSalt ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CC2=C3C(=C(C=C2S(=O)(=O)[O-])S(=O)(=O)[O-])C=CC4=C(C=C(C1=C43)S(=O)(=O)[O-])S(=O)(=O)[O-].[Na+].[Na+].[Na+].[Na+]
• Uses: Fluorescent probe.

Technology Process of 1,3,6,8-Pyrenetetrasulfonic acid, tetrasodium salt

There total 1 articles about 1,3,6,8-Pyrenetetrasulfonic acid, tetrasodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyrene (129-00-0) → tetrasodium pyrene-1,3,6,8-tetrasulphonate (59572-10-0)

Guidance literature:

pyrene; With sulfuric acid; at 90 ℃; for 1h;

With sulfur; at 40 - 100 ℃; for 8h; Concentration;

Reference yield: 71.0%

water (7732-18-5) + tetrasodium pyrene-1,3,6,8-tetrasulphonate (59572-10-0) + silver nitrate + triphenylphosphine (603-35-0) → [Ag4(1,3,6,8-pyrenetetrasulfonate)(triphenylphosphine)10]*8H2O

Guidance literature:

With aq. NH₃; In methanol; water; aq. soln. of NH3 added to mixt. of Na salt of ligand and AgNO3 in MeOH; PPh3 in MeOH added; heated and stirred for several min; filtered; filtrate evapd. in the dark for several d; recrystd. from MeOH; elem. anal.;

DOI:10.1016/j.molstruc.2005.11.003

Reference yield:

tetrasodium pyrene-1,3,6,8-tetrasulphonate (59572-10-0) → 8-hydroxy-1,3,6-pyrenetrisulfonic acid trisodium salt (6358-69-6)

Guidance literature:

With sodium hydroxide; In water; for 5h;

upstream raw materials:

pyrene

Downstream raw materials:

8-hydroxy-1,3,6-pyrenetrisulfonic acid trisodium salt

Refernces