1-CHLORO-2-IODOTETRAFLUOROETHANE

Base Information

• Chemical Name: 1-CHLORO-2-IODOTETRAFLUOROETHANE
• CAS No.: 421-78-3
• Molecular Formula: C2ClF4I
• Molecular Weight: 262.373
• Hs Code.: 2903799090
• Mol file: 421-78-3.mol

Synonyms:Ethane,1-chlorotetrafluoro-2-iodo- (6CI,7CI,8CI);1-Chloro-1,1,2,2-tetrafluoro-2-iodoethane;1-Chlorotetrafluoro-2-iodoethane;

Chemical Property of 1-CHLORO-2-IODOTETRAFLUOROETHANE

Chemical Property:

• Appearance/Colour: Colorless to pink Liquid
• Refractive Index: 1.392
• Boiling Point: 55.8 °C at 760 mmHg
• Flash Point: 56°C
• PSA: 0.00000
• Density: 2.309 g/cm³
• LogP: 2.84580
• Sensitive.: Light Sensitive

Purity/Quality:

98%min ^*data from raw suppliers

1-Chloro-2-iodotetrafluoroethane 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): T
• Hazard Codes: T
• Statements: 20/21/22-40
• Safety Statements: 23-36/37-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-CHLORO-2-IODOTETRAFLUOROETHANE

There total 1 articles about 1-CHLORO-2-IODOTETRAFLUOROETHANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

polytetrafluoroethylene (116-14-3,82785-14-6) → 1-chloro-1,1,2,2-tetrafluoro-2-iodo-ethane (421-78-3) + Pentafluoroethyl iodide (354-64-3)

Guidance literature:

With hydrogen fluoride; boron trifluoride; Iodine monochloride; at 25 ℃; for 18h; Product distribution; influence of the nature of catalyst, reaction time and temperature on the product distribution; further catalysts, further temperatures, further reaction times;

DOI:10.1021/jo961271o

Reference yield: 91.2%

1-chloro-1,1,2,2-tetrafluoro-2-iodo-ethane (421-78-3) → polytetrafluoroethylene (116-14-3,82785-14-6)

Guidance literature:

With sodium; ethyl acetoacetate; In ethanol; N,N-dimethyl-formamide; at 60 ℃; for 5h;

DOI:10.1016/S0022-1139(00)85017-4

Reference yield: 82.0%

1-chloro-1,1,2,2-tetrafluoro-2-iodo-ethane (421-78-3) + 2-allyl-4-pentenoic acid (99-67-2) → 6-(3-chloro-2,2,3,3-tetrafluoro-propyl)-3-oxa-bicyclo[3.2.1]octan-2-one

Guidance literature:

With sodium dithionite; sodium hydrogencarbonate; sodium hydroxide; In water; acetonitrile; at 20 ℃; for 6h; stereoselective reaction;

DOI:10.1016/j.tet.2010.07.002

upstream raw materials:

polytetrafluoroethylene

Downstream raw materials:

2-chloro-1,1,2,2-tetrafluoroethane

polytetrafluoroethylene

tetramethyl ethane-1,1,2,2-tetracarboxylate

3-Difluoromethyl-2,4-bis-methoxycarbonyl-pent-2-enedioic acid dimethyl ester

Refernces