1-(p-tolyl)-3-adamantanecarboxylicaci

Base Information

• Chemical Name: 1-(p-tolyl)-3-adamantanecarboxylicaci
• CAS No.: 56531-69-2
• Molecular Formula: C₁₈H₂₂O₂
• Molecular Weight: 270.371
• Hs Code.: 2916399090
• Mol file: 56531-69-2.mol

Synonyms:1-(p-tolyl)-3-adamantanecarboxylicaci;1-(p-Tolyl)-3-adamantanecarboxylic acid

Chemical Property of 1-(p-tolyl)-3-adamantanecarboxylicaci

Chemical Property:

• Vapor Pressure: 5.9E-08mmHg at 25°C
• Boiling Point: 424.3°Cat760mmHg
• Flash Point: 197.4°C
• PSA: 37.30000
• Density: 1.219g/cm³
• LogP: 3.91760
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

3-(4-Methylphenyl)adamantane-1-carboxylic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(p-tolyl)-3-adamantanecarboxylicaci

There total 1 articles about 1-(p-tolyl)-3-adamantanecarboxylicaci which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3-bromoadamantane-1-carboxylic acid (21816-08-0) + toluene (108-88-3,15644-74-3,16713-13-6) → 3-p-Tolyl-adamantane-1-carboxylic acid (56531-69-2)

Guidance literature:

With zinc(II) chloride; for 2h; Heating;

DOI:10.1016/j.bmcl.2007.02.057

Reference yield:

C9H17N3 (878218-09-8) + 3-p-Tolyl-adamantane-1-carboxylic acid (56531-69-2) → C27H37N3O

Guidance literature:

3-p-Tolyl-adamantane-1-carboxylic acid; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 60 ℃; for 1h;

C₉H₁₇N₃; In N,N-dimethyl-formamide; at 60 ℃; for 4h; Further stages.;

DOI:10.1016/j.bmcl.2007.02.057

Reference yield:

1-(phenylsulphonyl)piperazine (14172-55-5) + 3-p-Tolyl-adamantane-1-carboxylic acid (56531-69-2) → C28H34N2O3S

Guidance literature:

3-p-Tolyl-adamantane-1-carboxylic acid; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 60 ℃; for 1h;

1-(phenylsulphonyl)piperazine; In N,N-dimethyl-formamide; at 60 ℃; for 4h; Further stages.;

DOI:10.1016/j.bmcl.2007.02.057

upstream raw materials:

3-bromoadamantane-1-carboxylic acid

toluene

Downstream raw materials:

3-p-Tolyl-adamantane-1-carboxylic acid amide

1-chloro-3-p-tolyladamantane

Refernces