Technology Process of Allylbromomercury(II)
There total 3 articles about Allylbromomercury(II) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
acetone;
Sn(allyl)3(tr) was dissolved in acetone under Ar, solid HgBr2 was added and the mixt. refluxed gently overnight; Ar atm.;; solid Hg complex was filtered off after cooling, the filtrate was evapd. to dryness, the residue was stirred in CCl4, filtration, the filtrate was evapd., the residue was recrystd. from methanol; elem. anal.;
- Guidance literature:
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With
diethyl ether; bromine;
- Guidance literature:
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CH2=CHCH2MgX, HgBr2;