cyclohexane-1,3,5-triyltrimethanol

Base Information

• Chemical Name: cyclohexane-1,3,5-triyltrimethanol
• CAS No.: 5962-82-3
• Molecular Formula: C9H18O3
• Molecular Weight: 174.24
• Mol file: 5962-82-3.mol

Synonyms:

Chemical Property of cyclohexane-1,3,5-triyltrimethanol

Chemical Property:

• Vapor Pressure: 1.31E-05mmHg at 25°C
• Boiling Point: 329.5°Cat760mmHg
• Flash Point: 160.8°C
• Density: 1.074g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of cyclohexane-1,3,5-triyltrimethanol

There total 18 articles about cyclohexane-1,3,5-triyltrimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,3,5-triacetoxymethylcyclohexane (56025-62-8) → 1,3,5-trihydroxycyclohexane (5962-82-3)

Guidance literature:

With hydrogenchloride; water; In ethanol; Heating / reflux;

Reference yield: 89.0%

cis,cis-tri-n-propyl cyclohexane-1,3,5-tricarboxylate (107383-91-5) → cis,cis-1,3,5-tris(hydroxymethyl)cyclohexane (5962-82-3,72890-46-1)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; Reflux;

DOI:10.1039/c2dt12309f

Reference yield: 81.0%

cis,cis-triethyl 1,3,5-cyclohexanetricarboxylate (28084-34-6) → cis,cis-1,3,5-tris(hydroxymethyl)cyclohexane (5962-82-3,72890-46-1)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 16h; Heating;

DOI:10.1021/jo00385a002

upstream raw materials:

formaldehyd

2,4,6-Trinitrophenol

1,3,5-triacetoxymethylcyclohexane

trimethyl cis,cis-cyclohexane-1,3,5-tricarboxylate

Downstream raw materials:

1,3,5-tris-chloromethyl-cyclohexane

trivinyl ether of 1,3,5-cyclohexane-tris-methanol

1,3,5-tris-bromomethyl-cyclohexane

1r,3c,5c-tris-methanesulfonyloxymethyl-cyclohexane

Refernces

• 1、 Moriuchi, Toshiyuki,Mao, Lisheng,Wu, Hsyueh-Liang,Ohmura, Satoshi D.,Watanabe, Masami,Hirao, Toshikazu. "Synthesis of facial cyclometalated iridium(iii) complexes triggered by tripodal ligands". experimental part. p. 9519 - 9525. Retrieved 2012/09/11.
• 2、 -. "CONTRAST AGENTS". Page/Page column 17-18. . Retrieved 2008/06/13.