Technology Process of Naphthalene, 1-[(phenylmethyl)thio]-
There total 20 articles about Naphthalene, 1-[(phenylmethyl)thio]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
phenylmethanethiol;
With
sodium t-butanolate;
In
tetrahydrofuran;
at 23 ℃;
for 0.166667h;
Inert atmosphere;
With
zinc(II) chloride;
In
tetrahydrofuran;
for 0.166667h;
Inert atmosphere;
1-Bromonaphthalene;
With
di-μ-bromobis(tri-tert-butylphosphino)dipalladium(I); lithium iodide;
In
tetrahydrofuran;
at 90 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/jo900385d
- Guidance literature:
-
With
tetra(n-butyl)ammonium hydroxide;
In
water;
at 50 ℃;
for 24h;
chemoselective reaction;
Inert atmosphere;
Sealed tube;
DOI:10.1039/c2ob06795a
- Guidance literature:
-
With
trifluoromethylsulfonic anhydride; potassium iodide;
In
acetonitrile;
at 20 ℃;
for 0.05h;
DOI:10.1055/s-2008-1067190