Technology Process of 1,1'-(Hex-1-ene-1,2-diyl)dibenzene
There total 18 articles about 1,1'-(Hex-1-ene-1,2-diyl)dibenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(hex-1-yn-1-yl)benzene; phenylmagnesium bromide;
With
nickel(II) chloride hexahydrate;
In
tetrahydrofuran; toluene;
at 20 ℃;
for 1h;
Inert atmosphere;
Schlenk technique;
With
water;
In
tetrahydrofuran; toluene;
stereoselective reaction;
Inert atmosphere;
Schlenk technique;
DOI:10.1039/c3cc45202f
- Guidance literature:
-
With
bis(η3-allyl-μ-chloropalladium(II)); tetrabutyl ammonium fluoride; phosphorous acid trimethyl ester;
In
tetrahydrofuran;
at 50 ℃;
DOI:10.1039/b513528a
- Guidance literature:
-
n-butyllithium; diphenyl acetylene;
In
tetrahydrofuran; hexane;
at -10 ℃;
for 2h;
With
methanol;
In
tetrahydrofuran; hexane;
at -78 ℃;
DOI:10.1021/jo061949s