2,5-Cyclohexadien-1-one, 4,4'-[1,3-phenylenebis[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]meth ylidyne]]bis[2,6-bis(1,1-dimethylethyl)-

Base Information

• Chemical Name: 2,5-Cyclohexadien-1-one, 4,4'-[1,3-phenylenebis[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]meth ylidyne]]bis[2,6-bis(1,1-dimethylethyl)-
• CAS No.: 51062-61-4
• Molecular Formula: C₆₄H₈₆O₄
• Molecular Weight: 919.384
• Mol file: 51062-61-4.mol

Synonyms:

Chemical Property of 2,5-Cyclohexadien-1-one, 4,4'-[1,3-phenylenebis[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]meth ylidyne]]bis[2,6-bis(1,1-dimethylethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-Cyclohexadien-1-one, 4,4'-[1,3-phenylenebis[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]meth ylidyne]]bis[2,6-bis(1,1-dimethylethyl)-

There total 2 articles about 2,5-Cyclohexadien-1-one, 4,4'-[1,3-phenylenebis[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]meth ylidyne]]bis[2,6-bis(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromo-2,6-di-tert-butylphenol (1139-52-2) → m-Bisbenzene (51062-61-4)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) nBuLi, THF, hexane, (ii) /BRN= 1209232/

2: (i) nBuLi, Me₂NCH₂CH₂NMe₂, THF, hexane, (ii) /BRN= 2052705/, (iii) aq. HCl

DOI:10.1016/0040-4020(75)85041-1

Reference yield:

diethyl isophthalate (636-53-3) + (4-Bromo-2,6-di-tert-butylphenoxy)trimethylsilane (27329-74-4) → m-Bisbenzene (51062-61-4)

Guidance literature:

Multistep reaction; (i) nBuLi, Me₂NCH₂CH₂NMe₂, THF, hexane, (ii) /BRN= 2052705/, (iii) aq. HCl;

DOI:10.1016/0040-4020(75)85041-1

Reference yield:

m-Bisbenzene (51062-61-4) → m-Phenylenebis(galvinoxyl) biradical (51062-64-7)

Guidance literature:

With potassium hydroxide; potassium hexacyanoferrate(III); In diethyl ether;

DOI:10.1016/0040-4020(75)85041-1

upstream raw materials:

diethyl isophthalate

(4-Bromo-2,6-di-tert-butylphenoxy)trimethylsilane

4-bromo-2,6-di-tert-butylphenol

Downstream raw materials:

m-Phenylenebis(galvinoxyl) biradical