Triaminoguanidine mononitrate

Base Information

• Chemical Name: Triaminoguanidine mononitrate
• CAS No.: 4000-16-2
• Deprecated CAS: 116753-68-5
• Molecular Formula: CH8N6•NO3
• Molecular Weight: 167.128
• European Community (EC) Number: 223-647-2
• UNII: T9867X3GPS
• DSSTox Substance ID: DTXSID60481215
• Mol file: 4000-16-2.mol

Synonyms:Triaminoguanidine mononitrate;UNII-T9867X3GPS;T9867X3GPS;Carbonohydrazonic dihydrazide, mononitrate;Carbonohydrazonic dihydrazide, nitrate (1:1);GUANIDINE, 1,2,3-TRIAMINO-, MONONITRATE;1,2,3-Triaminoguanidinium mononitrate;57931-27-8;HSDB 7166;DTXSID60481215;EINECS 223-647-2;AKOS024343422;TRIAMINOGUANIDINE NITRATE [HSDB];CARBOHYDRAZIDE, HYDRAZONE, MONONITRATE;GUANIDINE, 1,2,3-TRIAMINO-, NITRATE

Chemical Property of Triaminoguanidine mononitrate

Chemical Property:

• Vapor Pressure: 1.18E-06mmHg at 25°C
• Boiling Point: 290.7°Cat760mmHg
• Flash Point: 129.6°C
• PSA: 183.23000
• Density: g/cm³
• LogP: 0.20090
• Hydrogen Bond Donor Count: 6
• Hydrogen Bond Acceptor Count: 7
• Rotatable Bond Count: 2
• Exact Mass: 167.07668717
• Heavy Atom Count: 11
• Complexity: 83.3

Purity/Quality:

99% ^*data from raw suppliers

NITRIC ACID COMPOUND WITH HYDRAZINECARBOHYDRAZONOHYDRAZIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(=NN)(NN)NN.[N+](=O)(O)[O-]

Technology Process of Triaminoguanidine mononitrate

There total 2 articles about Triaminoguanidine mononitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

guanidine hydrogen carbonate (124-46-9,20734-13-8,100224-74-6,593-85-1,90332-86-8,3425-08-9) → 1,2,3-triaminoguanidinium nitrate (4000-16-2)

Guidance literature:

guanidine hydrogen carbonate; With nitric acid; In water;

With hydrazine; In 1,4-dioxane;

DOI:10.1002/chem.201500982

Reference yield: 83.0%

guanidine nitrate (506-93-4) → 1,2,3-triaminoguanidinium nitrate (4000-16-2)

Guidance literature:

With nitric acid; hydrazine hydrate; In water; at 90 - 98 ℃; for 1h; pH=7; Temperature;

Reference yield: 83.0%

1,2,3-triaminoguanidinium nitrate (4000-16-2) + acetylacetone (123-54-6,81235-32-7) → 3,6-bis(3,5-dimethyl-1H-pyrazol-1-yl)-1,4-dihydro-1,2,4,5-tetrazine (30169-21-2)

Guidance literature:

In water; at 60 - 70 ℃; for 4.5h;

DOI:10.1007/s10870-012-0287-8

upstream raw materials:

guanidine hydrogen carbonate

guanidine nitrate

Downstream raw materials:

3,6-bis(3,5-dimethyl-1H-pyrazol-1-yl)-1,4-dihydro-1,2,4,5-tetrazine

Refernces

• 1、 -. "Synthesis method of triaminoguanidinium nitrate". Paragraph 0021; 0022; 0023; 0024. . Retrieved 2016/10/08.