METHYL 10-METHYLUNDECANOATE

Base Information

• Chemical Name: METHYL 10-METHYLUNDECANOATE
• CAS No.: 5129-56-6
• Molecular Formula: C13H26O2
• Molecular Weight: 214.348
• Hs Code.: 2915900090
• Mol file: 5129-56-6.mol

Synonyms:Methyl isolaurate;10-Methyl-undecansaeure-methylester;Methyl 10-methylundecanoate;methyl 10-undecanoate;methyl 10-methyl-undecanoate;10-methyl-undecanoic acid methyl ester;Undecanoic acid,10-methyl-,methyl ester;

Chemical Property of METHYL 10-METHYLUNDECANOATE

Chemical Property:

• Vapor Pressure: 0.0236mmHg at 25°C
• Boiling Point: 248.9oC at 760mmHg
• Flash Point: 104.7oC
• PSA: 26.30000
• Density: 0.867 g/cm3
• LogP: 3.93620
• Storage Temp.: 2-8°C

Purity/Quality:

95% ^*data from raw suppliers

METHYL-10-METHYLUNDECANOATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of METHYL 10-METHYLUNDECANOATE

There total 1 articles about METHYL 10-METHYLUNDECANOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C61H107NO19 + diazomethyl-trimethyl-silane (18107-18-1) → methyl heptanoate (106-73-0) + methyl octanate (111-11-5) + Methyl decanoate (110-42-9) + methyl undecanoate (1731-86-8) + undecanoic acid, 10-methyl-, methyl ester (5129-56-6) + methyl 6-methylheptanoate (2519-37-1)

Guidance literature:

C₆₁H₁₀₇NO₁₉; With hydrogenchloride; methanol; at 80 ℃; for 12h; Sealed tube;

With potassium permanganate; sodium periodate; potassium carbonate; In tert-butyl alcohol; at 37 ℃; for 18h;

diazomethyl-trimethyl-silane; Further stages;

DOI:10.1016/j.bmc.2011.06.051

Reference yield: 100.0%

undecanoic acid, 10-methyl-, methyl ester (5129-56-6) → 10-methyl-1-undecanol (20194-45-0)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 2.5h;

DOI:10.1021/np010307r

Reference yield:

undecanoic acid, 10-methyl-, methyl ester (5129-56-6) → C25H42O2 (942137-21-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 95 percent / LAH / diethyl ether / Heating

2: 91 percent / Ph₃P; Br₂; pyridine / CH₂Cl₂

3: 84 percent / Mg; CuBr / tetrahydrofuran / -78 °C

With pyridine; lithium aluminium tetrahydride; bromine; magnesium; triphenylphosphine; copper(I) bromide; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1016/j.tetlet.2007.03.115

upstream raw materials:

diazomethyl-trimethyl-silane

Downstream raw materials:

10-methyl-1-undecanol

C₂₅H₄₂O₂

C₂₅H₄₂O

1-bromo-10-methylundecane

Refernces