Technology Process of Benzene, (2-methyl-2-nitrosopropyl)-
There total 6 articles about Benzene, (2-methyl-2-nitrosopropyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 2 steps
1: 3N HCl / ethanol / electrochemical reduction (1.20 V, Hg cathode, SCE)
2: H2O / 25 °C / buffer of pH 8.8, controlled potential electrolysis; further N-alkylhydroxylamines without a β-hydroxy group
With
hydrogenchloride;
In
ethanol; water;
- Guidance literature:
-
With
hydrogenchloride; sodium tungstate; dihydrogen peroxide;
Yield given. Multistep reaction;
1.) reflux, 1 h;
- Guidance literature:
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Multi-step reaction with 2 steps
1: 55 percent / conc. sulfuric acid, glacial acetic acid / 1.) 75 deg C, 30 min, 2.) room temerpature, 2 h
2: 1.) aq. HCl, 2.) sodium tungstate, hydrogen peroxide / 1.) reflux, 1 h
With
hydrogenchloride; sodium tungstate; sulfuric acid; dihydrogen peroxide; acetic acid;