Technology Process of Octaborane(8), octachloro-
There total 3 articles about Octaborane(8), octachloro- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
tetrachloromethane;
100°C, 2 weeks; NMR monitoring; not isolated, detected by NMR;
DOI:10.1021/ja00388a057
- Guidance literature:
-
In
trichlorofluoromethane;
byproducts: CCl4; B2Cl4 and 10-fold excess CCl3F were heated in a sealed tube at 90°C for 61 h; partially septd. by fractionation at -95 to -160°C; products detected by (19)F- and (11)B-NMR, CCl4 by (13)C-NMR;
- Guidance literature:
-
In
neat (no solvent);
byproducts: BCl3; at 60°C for 24 h; cyclohexane condensed; filtered; evapd.; at 45°C for 24 h; monitored by (11)B NMR;