Tris(acetyloxy)(4-fluorophenyl)plumbane

Base Information Edit

Chemical Name:Tris(acetyloxy)(4-fluorophenyl)plumbane
CAS No.:53243-78-0
Molecular Formula:C12H13FO6Pb
Molecular Weight:479.43
Hs Code.:
DSSTox Substance ID:DTXSID70587015
Wikidata:Q82479249
Mol file:53243-78-0.mol

Synonyms:53243-78-0;Tris(acetyloxy)(4-fluorophenyl)plumbane;DTXSID70587015

Suppliers and Price of Tris(acetyloxy)(4-fluorophenyl)plumbane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tris(acetyloxy)(4-fluorophenyl)plumbane Edit

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:480.04627
Heavy Atom Count:20
Complexity:351

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)O[Pb](C1=CC=C(C=C1)F)(OC(=O)C)OC(=O)C

Technology Process of Tris(acetyloxy)(4-fluorophenyl)plumbane

There total 2 articles about Tris(acetyloxy)(4-fluorophenyl)plumbane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: lead(IV) acetate

: 17151-47-2
tributyl(4-fluorophenyl)stannane

: 53243-78-0
p-Fluorophenyl-lead triacetate

Guidance literature:: mercury(II) trifluoroacetate; In chloroform; byproducts: Bu3SnOAc; stirred at 40°C for 20 h;; filtered through Celite; solvent removed; light petroleum added; ppt. washed with light petroleum; crystd. from CHCl3/light petroleum;;

Reference yield: 74.0%

: lead(IV) tetraacetate

: 17151-47-2
tributyl(4-fluorophenyl)stannane

: 13257-51-7
mercury(II) trifluoroacetate

: 53243-78-0
4-fluorophenyllead triacetate

Guidance literature:: In chloroform; addn. of Sn-compd. and Hg(OOCCF3) to a soln. of Pb(OAc)4 in CHCl3, stirring at 40°C overnight; filtration (Kieselgur), evapn. of filtrate (vac., 40°C), dissoln. of oily residue in petroleum ether (40-60°C), crystn. on storing in refrigerator, recrystn. from CHCl3/petroleum ether; elem. anal.;
DOI:10.1016/0022-328X(92)83382-R