Methanone, (4-methoxyphenyl)[(1R,2R)-2-phenylcyclopropyl]-, rel-

Base Information Edit

Chemical Name:Methanone, (4-methoxyphenyl)[(1R,2R)-2-phenylcyclopropyl]-, rel-
CAS No.:54619-93-1
Molecular Formula:C17H16O2
Molecular Weight:252.313
Hs Code.:
Mol file:54619-93-1.mol

Synonyms:

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Chemical Property of Methanone, (4-methoxyphenyl)[(1R,2R)-2-phenylcyclopropyl]-, rel- Edit

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Methanone, (4-methoxyphenyl)[(1R,2R)-2-phenylcyclopropyl]-, rel-

There total 2 articles about Methanone, (4-methoxyphenyl)[(1R,2R)-2-phenylcyclopropyl]-, rel- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1774-47-6
trimethylsulfoxonium iodide

: 959-23-9
4'-methoxychalcone

: 54619-93-1
(4-methoxyphenyl)(2-phenylcyclopropyl)methanone

Guidance literature:: trimethylsulfoxonium iodide; With sodium hydride; In dimethyl sulfoxide; mineral oil; at 20 ℃; for 0.25h; Inert atmosphere;

4'-methoxychalcone; In dimethyl sulfoxide; mineral oil; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1039/d0cc05167e

Reference yield: 70.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 54619-93-1
(4-methoxyphenyl)(2-phenylcyclopropyl)methanone

Guidance literature:: With oxygen; copper diacetate; palladium diacetate; at 100 ℃;
DOI:10.1002/anie.201408245

Reference yield: 89.0%

: 54619-93-1
(4-methoxyphenyl)(2-phenylcyclopropyl)methanone

: 536-74-3
phenylacetylene

: C₂₅H₂₂O₂

Guidance literature:: phenylacetylene; With ethylmagnesium bromide; In tetrahydrofuran; at 50 ℃; for 1h;

(4-methoxyphenyl)(2-phenylcyclopropyl)methanone; In tetrahydrofuran; at 23 - 25 ℃; for 3h; Further stages.;
DOI:10.1039/b714511j