Platinum, bis(tricyclohexylphosphine)-

Base Information Edit

Chemical Name:Platinum, bis(tricyclohexylphosphine)-
CAS No.:55664-33-0
Molecular Formula:C36H66P2Pt
Molecular Weight:755.948
Hs Code.:
Mol file:55664-33-0.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Platinum, bis(tricyclohexylphosphine)- Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Platinum, bis(tricyclohexylphosphine)-

There total 20 articles about Platinum, bis(tricyclohexylphosphine)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 12130-66-4
bis(cycloocta-1,5-diene)platinum⁽⁰⁾

: 2622-14-2
tricyclohexylphosphine

: 55664-33-0
bis(tricyclohexylphosphine)platinum⁽⁰⁾

Guidance literature:: In Petroleum ether; N2-atmosphere; addn. of 2 equiv. of phosphine to suspn. of Pt-complex; pptn. on concn. (reduced pressure), decantation, washing (light petroleum), recrystn. (light petroleum); elem. anal.;
DOI:10.1039/DT9770001006

Reference yield: 55.0%

: 60158-99-8,105762-06-9
PtCl₂(PCy₃)2

: 55664-33-0
bis(tricyclohexylphosphine)platinum⁽⁰⁾

Guidance literature:: With potassium graphite; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1021/acs.organomet.6b00924

Reference yield: 39.0%

: [Pt(allyl)Cl]4

: 2622-14-2
tricyclohexylphosphine

: 55664-33-0
bis(tricyclohexylphosphine)platinum⁽⁰⁾

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; hetead under N2 to 65°C overnight, then cooled to room temp.; THF evapd. in vac., the residue dried heating with warm water for 2 h, the residue extd. with warm heptane, filtered, pptn. by slow cooling to room temp., heptane siphoned off, the crystals washed with pentane and dried in vac.; elem. anal.;
DOI:10.1039/DT9800000776