Technology Process of Thiocyanic acid, 2,4,6-trimethylphenyl ester
There total 15 articles about Thiocyanic acid, 2,4,6-trimethylphenyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,3,5-trimethyl-2-(methylsulfinyl)benzene;
With
trifluoromethylsulfonic anhydride;
In
dichloromethane;
at -78 ℃;
for 0.0833333h;
Inert atmosphere;
trimethylsilyl cyanide;
In
dichloromethane;
at -78 - 23 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/acs.orglett.1c00460
- Guidance literature:
-
With
N,N'-dibromo-N,N'-1,2-ethylene bis(2,5-dimethylbenzene sulfonamide);
In
methanol;
at 0 ℃;
for 2h;
DOI:10.3390/60300253
- Guidance literature:
-
With
copper(II) acetate monohydrate;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1002/chem.201806261
