Technology Process of Acetyl chloride, [[(4-methylphenyl)sulfonyl]amino]-
There total 3 articles about Acetyl chloride, [[(4-methylphenyl)sulfonyl]amino]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
thionyl chloride;
for 1.5h;
Heating / reflux;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydrogencarbonate / water / 0.33 h / 0 °C / Inert atmosphere
1.2: 16 h / Inert atmosphere; Sealed tube
2.1: thionyl chloride / tetrahydrofuran / 1 h / 0 - 23 °C / Inert atmosphere; Sealed tube
With
thionyl chloride; sodium hydrogencarbonate;
In
tetrahydrofuran; water;
DOI:10.1021/acs.orglett.5b03708
- Guidance literature:
-
With
Dichloromethyl methyl ether;