Nonanal, 7-methyl-

Base Information

• Chemical Name: Nonanal, 7-methyl-
• CAS No.: 58223-46-4
• Molecular Formula: C10H20O
• Mol file: 58223-46-4.mol

Synonyms:

Chemical Property of Nonanal, 7-methyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Nonanal, 7-methyl-

There total 16 articles about Nonanal, 7-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.4%

7-methyl-nonan-1-ol (33234-93-4) → 7-methylnonanal (58223-46-4)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; for 4h;

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) → 7-methylnonanal (58223-46-4)

Guidance literature:

Multi-step reaction with 5 steps

1: Br₂ / diethyl ether / -10 - 0 °C

2: 28 percent / diethyl ether / 12 h / Ambient temperature

3: 66 percent / Na / diethyl ether / 3 h / Heating

4: 94 percent / H₂ / 10percent Pd/C / ethyl acetate

5: 84.4 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h

With hydrogen; bromine; sodium; pyridinium chlorochromate; palladium on activated charcoal; In diethyl ether; dichloromethane; ethyl acetate;

Reference yield:

2,3-dibromotetrahydropyran (56660-59-4) → 7-methylnonanal (58223-46-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 28 percent / diethyl ether / 12 h / Ambient temperature

2: 66 percent / Na / diethyl ether / 3 h / Heating

3: 94 percent / H₂ / 10percent Pd/C / ethyl acetate

4: 84.4 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h

With hydrogen; sodium; pyridinium chlorochromate; palladium on activated charcoal; In diethyl ether; dichloromethane; ethyl acetate;

upstream raw materials:

7-methyl-nonan-1-ol

(6-bromohexyl)-trimethylsilyl ether

trimethyl-(7-methyl-nonyloxy)-silane

3,4-dihydro-2H-pyran

Refernces

• 1、 Pojar-Fene?an, Maria,Oprean, Ion,Pop, Lidia M.,Balea, Ana. "Exo- and endohormones. XVIII. Synthesis of racemic 8-methyl-2-decyl propanoate, the sex pheromone of western corn rootworm Diabrotica virgifera virgifera LeConte (Coleoptera, Chrisomelidae)". . p. 263 - 266. Retrieved 2007/10/03.