Technology Process of 5-Methyl-10-phenyl-10-oxo-5,10-dihydrophenophosphazine
There total 15 articles about 5-Methyl-10-phenyl-10-oxo-5,10-dihydrophenophosphazine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,4-diaza-bicyclo[2.2.2]octane; tetrabutylammonium tetrafluoroborate;
In
water; acetonitrile;
at 25 ℃;
for 10.73h;
Inert atmosphere;
Electrochemical reaction;
DOI:10.1021/acs.orglett.1c00807
- Guidance literature:
-
With
tris-(trimethylsilyl)silane; palladium diacetate;
In
N,N-dimethyl-formamide;
at 130 ℃;
for 12h;
Inert atmosphere;
Sealed tube;
DOI:10.1021/ol503252t
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dimethyl sulfoxide / 3 h / Inert atmosphere; Sealed tube
2: iron; ammonium chloride / ethanol; water / 3 h / Sealed tube; Reflux
3: sodium nitrite; potassium iodide; toluene-4-sulfonic acid / water; acetonitrile / 0 - 20 °C / Sealed tube
4: copper(l) iodide; caesium carbonate / toluene / 48 h / 110 °C / Sealed tube; Inert atmosphere
5: tris-(trimethylsilyl)silane; palladium diacetate / N,N-dimethyl-formamide / 12 h / 130 °C / Inert atmosphere; Sealed tube
6: tris-(trimethylsilyl)silane; palladium diacetate / N,N-dimethyl-formamide / 12 h / 130 °C / Inert atmosphere; Sealed tube
With
copper(l) iodide; tris-(trimethylsilyl)silane; palladium diacetate; iron; ammonium chloride; caesium carbonate; toluene-4-sulfonic acid; potassium iodide; sodium nitrite;
In
ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ol503252t