7H-Benzo[c]carbazole

Base Information

• Chemical Name: 7H-Benzo[c]carbazole
• CAS No.: 205-25-4
• Molecular Formula: C16H11N
• Molecular Weight: 217.27
• Hs Code.: 2933990090
• European Community (EC) Number: 205-909-8
• NSC Number: 108995
• UNII: J2W3Z6C2NQ
• DSSTox Substance ID: DTXSID00174477
• Nikkaji Number: J193.678F
• Wikidata: Q72445366
• Mol file: 205-25-4.mol

Synonyms:7H-Benzo[c]carbazole;205-25-4;3,4-Benzocarbazole;7H-Benzo(c)carbazole;7-Aza-7H-benzo(c)fluorene;7-Aza-7H-benzo[c]fluorene;J2W3Z6C2NQ;EINECS 205-909-8;NSC 108995;NSC-108995;NSC108995;UNII-J2W3Z6C2NQ;7H-benzo[c]carbazole, 99%;SCHEMBL257083;DTXSID00174477;MFCD00215940;AKOS016014045;DS-6627;OL10196;SB66347;B5590;CS-0095315;FT-0717100;F13520;A846259

Chemical Property of 7H-Benzo[c]carbazole

Chemical Property:

• Vapor Pressure: 4.5E-08mmHg at 25°C
• Melting Point: 135-137 °C
• Refractive Index: 1.822
• Boiling Point: 456.116 °C at 760 mmHg
• PKA: 17.00±0.30(Predicted)
• Flash Point: 207.893 °C
• PSA: 15.79000
• Density: 1.277 g/cm³
• LogP: 4.47430
• Storage Temp.: Sealed in dry,Room Temperature
• XLogP3: 5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 217.089149355
• Heavy Atom Count: 17
• Complexity: 287

Purity/Quality:

98%,99%, ^*data from raw suppliers

[c]-Benzocarbazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=CC3=C2C4=CC=CC=C4N3

Technology Process of 7H-Benzo[c]carbazole

There total 88 articles about 7H-Benzo[c]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.7%

2-nitro-1-phenylnaphthalene (92795-22-7) → benzo[c]carbazole (205-25-4)

Guidance literature:

With iron; triphenylphosphine; In toluene; at 106 ℃; for 10h;

Reference yield: 96.0%

5,6-dihydro-7H-benzocarbazole (5425-53-6) → benzo[c]carbazole (205-25-4)

Guidance literature:

With chloranil; In xylene; for 2h; Inert atmosphere; Reflux;

Reference yield: 96.0%

5,6-dihydro-11H-benzo[a]carbazole (21064-49-3) → benzo[c]carbazole (205-25-4)

Guidance literature:

With chloranil; In 5,5-dimethyl-1,3-cyclohexadiene; for 2h; Reflux; Inert atmosphere;

upstream raw materials:

5,6-dihydro-7H-benzocarbazole

1-(naphthalen-2-yl)-1H-benzo[d][1,2,3]triazole

7,8,9,11-tetrahydrobenzo[c]carbazole

3-phenyl-3H-naphtho[1,2-d][1,2,3]triazole

Downstream raw materials:

C₃₇H₂₄N₂

C₃₇H₂₃BrN₂

C₅₅H₃₈N₂Si

C₂₅H₁₅ClN₂

Refernces

• 1、 Clemo,Felton. "-". . p. 1658,1667. Retrieved 1952.
• 2、 Gao, Hongyin,Liu, Fengting,Lu, Haifeng,Qu, Jiatong,Wang, Min. "Synthesis of non-C2symmetrical NOBIN-type biaryls through a cascade N -arylation and [3,3]-sigmatropic rearrangement from O -arylhydroxylamines and diaryliodonium salts". supporting information. p. 7246 - 7251. Retrieved 2021/08/30.
• 3、 -. "COMPOUND FOR ORGANIC ELECTRONIC ELEMENT, ORGANIC ELECTRONIC ELEMENT USING THE SAME, AND AN ELECTRONIC DEVICE THEREOF". Paragraph 0525; 0538-0540; 0547; 0548. . Retrieved 2020/05/26.