chrysazol

Base Information

• Chemical Name: chrysazol
• CAS No.: 607-61-4
• Molecular Formula: C14H10O2
• Molecular Weight: 210.22800
• Hs Code.: 2907299090
• Mol file: 607-61-4.mol

Synonyms:1,8-anthradiol;1,8-Anthracenediol;Anthracen-1,8-diol;1,8-Anthracendiol;1.8-Dioxy-anthracen;1,8-dihydroxyanthracene;

Chemical Property of chrysazol

Chemical Property:

• PSA: 40.46000
• LogP: 3.40420

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of chrysazol

There total 8 articles about chrysazol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

anthracene-1,8-disulphonic acid (61736-92-3) → 1,8-dihydroxyanthraquinone (607-61-4)

Guidance literature:

With potassium hydroxide; Heating;

Reference yield: 84.0%

1,8-dimethoxyanthracene (16294-34-1) → 1,8-dihydroxyanthraquinone (607-61-4)

Guidance literature:

With boron tribromide; In dichloromethane;

DOI:10.1016/j.tetlet.2004.06.135

Reference yield:

1,8-diacetoxy-9,10-anthraquinone (1963-82-2) → 1,8-dihydroxy-9,10-dihydroanthracene (64817-82-9) + 1,8-dihydroxyanthraquinone (607-61-4)

Guidance literature:

1,8-diacetoxy-9,10-anthraquinone; With acetic acid; zinc; at 135 ℃;

With pyridine; acetyl chloride; at 0 - 20 ℃;

With methylamine; In methanol; dichloromethane; at 0 - 20 ℃;

DOI:10.1055/s-2008-1078499

upstream raw materials:

anthracene-1,8-disulphonic acid

1,8-dimethoxyanthracene

anthracene

1,8-diacetoxy-9,10-anthraquinone

Downstream raw materials:

1,8-diacetoxyanthracene

Refernces

• 1、 Tang, Bo,Yang, Hong-Mei,Hu, Wen-Jing,Ma, Ming-Liang,Liu, Yahu A.,Li, Jiu-Sheng,Jiang, Biao,Wen, Ke. "1,8-Dioxyanthracene-Derived Crown Ethers: Synthesis, Complexation with Paraquat and Assembly of a Tetracationic Cyclophane-Crown Ether Based [2]Catenane". . p. 6925 - 6934. Retrieved 2016/02/19.
• 2、 Quast, Helmut,Fuchsbauer, Hans-Lothar. "ESR Spectroscopic Detection of Intramolecular Interactions in Radical Cations of Poly(α-methoxy)triptycenes". . p. 1016 - 1038. Retrieved 2007/10/02.