Technology Process of 2,2,4,4,6,6,8,8,10,10,12,12,14,14-tetradecachloro-2lambda~5~,4lambda~5~,6lambda~5~,8lambda~5~,10lambda~5~,12lambda~5~,14lambda~5~-cycloheptaphosphaza-1,3,5,7,9,11,13-heptaene
There total 2 articles about 2,2,4,4,6,6,8,8,10,10,12,12,14,14-tetradecachloro-2lambda~5~,4lambda~5~,6lambda~5~,8lambda~5~,10lambda~5~,12lambda~5~,14lambda~5~-cycloheptaphosphaza-1,3,5,7,9,11,13-heptaene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
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-
940-71-6,16422-79-0
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine
- Guidance literature:
-
In
chlorobenzene;
Schlenk technique;
Reflux;
DOI:10.1021/ic500272b
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-
940-71-6,16422-79-0
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine
- Guidance literature:
-
With
quinoline;
In
further solvent(s);
heating a soln. of PCl5 in (CHCl2)2 with quinoline at 145 °C on refluxing;; distn. off solvent; formation of a mixt. of 40 % (NPCl2)3, 55-60 % (PNCl2)7 and 0-5 % impurities;;
- Guidance literature:
-
With
potassium hydride;
In
tetrahydrofuran;
Glovebox;
Schlenk technique;
Inert atmosphere;
Reflux;
DOI:10.1021/ic500272b