4-Phenoxybenzene-1-diazonium chloride

Base Information

• Chemical Name: 4-Phenoxybenzene-1-diazonium chloride
• CAS No.: 6099-72-5
• Molecular Formula: C12H9N2O.Cl
• Molecular Weight: 232.669
• DSSTox Substance ID: DTXSID30504440
• Mol file: 6099-72-5.mol

Synonyms:4-Phenoxybenzene-1-diazonium chloride;6099-72-5;SCHEMBL3796451;DTXSID30504440

Chemical Property of 4-Phenoxybenzene-1-diazonium chloride

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 232.0403406
• Heavy Atom Count: 16
• Complexity: 231

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)OC2=CC=C(C=C2)[N+]#N.[Cl-]

Technology Process of 4-Phenoxybenzene-1-diazonium chloride

There total 1 articles about 4-Phenoxybenzene-1-diazonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-phenoxyanilin (139-59-3) → 4-Phenoxy-benzoldiazonium-chlorid (6099-72-5)

Guidance literature:

With sodium nitrite; In hydrogenchloride;

DOI:10.1002/omr.1270210710

Reference yield: 77.0%

4-Phenoxy-benzoldiazonium-chlorid (6099-72-5) + Sodium; [6,6-dimethyl-4-oxo-dihydro-pyran-(3Z)-ylidene]-methanolate → 2,2-dimethyl-5-[(4-phenoxy-phenyl)hydrazono]-tetrahydro-pyran-4-one

Guidance literature:

In water; at -5 - 0 ℃; for 1h;

DOI:10.1016/S0968-0896(02)00176-1

Reference yield:

4-Phenoxy-benzoldiazonium-chlorid (6099-72-5) → 1-azido-4-phenoxybenzene (85862-67-5)

Guidance literature:

With sodium azide; In water; at 20 ℃; for 1h;

DOI:10.2174/1573406411309040004

upstream raw materials:

4-phenoxyanilin

Downstream raw materials:

4-Phenoxyphenylhydrazine

Refernces

• 1、 Utsintong, Maleeruk,Massarotti, Alberto,Caldarelli, Antonio,Theeramunkong, Sewan. "Parallel synthesis of "Click" chalcones as antitubulin agents". . p. 510 - 516. Retrieved 2013/07/28.
• 2、 Dunn, III, W.J.,Lins, C.,Kumar, G.,Manimaran, T.,Grigoras, S.,et al.. "Substituent Effects on 13C and 15N Chemical Shifts in Triazenes Studied by Principal Components Multivariate Data Analysis". . p. 450 - 456. Retrieved 2007/10/02.