Isoquinolinium, 1-cyano-2-oxo-2-phenylethylide

Base Information

• Chemical Name: Isoquinolinium, 1-cyano-2-oxo-2-phenylethylide
• CAS No.: 61095-44-1
• Molecular Formula: C₁₈H₁₂N₂O
• Molecular Weight: 272.306
• Mol file: 61095-44-1.mol

Synonyms:

Chemical Property of Isoquinolinium, 1-cyano-2-oxo-2-phenylethylide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Isoquinolinium, 1-cyano-2-oxo-2-phenylethylide

There total 3 articles about Isoquinolinium, 1-cyano-2-oxo-2-phenylethylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-isoquinolinio-acetoxycarbonylcyanomethylide (96284-58-1) → 2-isoquinolinio-benzoylcyanomethylide (50737-39-8,61095-44-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 35 percent / 30 percent H₂O₂ / acetic acid / 3 h / Heating

2: 34.9 percent / acetic anhydride; dimethylformamide / 1 h; RT, 2 h

With dihydrogen peroxide; In acetic anhydride; acetic acid; N,N-dimethyl-formamide;

Reference yield:

2-isoquinolinio-acetylcyanomethylide → 2-isoquinolinio-benzoylcyanomethylide (50737-39-8,61095-44-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 58 percent / 30 percent H₂O₂ / acetic acid / 3 h / Heating

2: 34.9 percent / acetic anhydride; dimethylformamide / 1 h; RT, 2 h

With dihydrogen peroxide; In acetic anhydride; acetic acid; N,N-dimethyl-formamide;

Reference yield:

→ 2-isoquinolinio-benzoylcyanomethylide (50737-39-8,61095-44-1)

Guidance literature:

Aus 16 + Isochinolin;

DOI:10.1021/ja00434a044

upstream raw materials:

2-isoquinolinio-acetoxycarbonylcyanomethylide

Refernces