Technology Process of Benzene, 1-iodo-2-(1-methylethenyl)-
There total 8 articles about Benzene, 1-iodo-2-(1-methylethenyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Methyltriphenylphosphonium bromide;
With
potassium tert-butylate;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Schlenk technique;
Inert atmosphere;
2-iodoacetophenone;
In
tetrahydrofuran;
for 12h;
Schlenk technique;
Inert atmosphere;
- Guidance literature:
-
With
potassium tert-butylate; Methyltriphenylphosphonium bromide;
In
tetrahydrofuran;
at 0 - 22 ℃;
for 16h;
Inert atmosphere;
Schlenk technique;
DOI:10.1055/s-0036-1590967
- Guidance literature:
-
1-bromo-2-isopropenylbenzene;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.5h;
Inert atmosphere;
With
iodine;
In
tetrahydrofuran; hexane;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/jo501383v