Cyclohexaneethanol, 4-(1,1-dimethylethyl)-, trans-

Base Information

• Chemical Name: Cyclohexaneethanol, 4-(1,1-dimethylethyl)-, trans-
• CAS No.: 61244-90-4
• Molecular Formula: C₁₂H₂₄O
• Molecular Weight: 184.322
• Mol file: 61244-90-4.mol

Synonyms:

Chemical Property of Cyclohexaneethanol, 4-(1,1-dimethylethyl)-, trans-

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexaneethanol, 4-(1,1-dimethylethyl)-, trans-

There total 3 articles about Cyclohexaneethanol, 4-(1,1-dimethylethyl)-, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-tercbutyl-cyclohexanone (98-53-3) → 2-(4-tert-Butyl-cyclohexyl)-ethanol (61244-90-4)

Guidance literature:

Multi-step reaction with 3 steps

1: MeONa / petroleum ether

2: H₂ / 5 percent Pd/C / ethyl acetate

3: LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; hydrogen; sodium methylate; palladium on activated charcoal; In diethyl ether; ethyl acetate; Petroleum ether;

DOI:10.1002/hlca.19830660503

Reference yield:

methyl 4-tert-butylcyclohexylideneacetate (88166-26-1,100281-94-5,85048-20-0) → 2-(4-tert-Butyl-cyclohexyl)-ethanol (61244-90-4)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / 5 percent Pd/C / ethyl acetate

2: LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; ethyl acetate;

DOI:10.1002/hlca.19830660503

Reference yield:

methyl trans-(4-t-butylcyclohexyl)acetate (28125-17-9) → 2-(4-tert-Butyl-cyclohexyl)-ethanol (61244-90-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1002/hlca.19830660503

upstream raw materials:

methyl trans-(4-t-butylcyclohexyl)acetate

4-tercbutyl-cyclohexanone

methyl 4-tert-butylcyclohexylideneacetate

Downstream raw materials:

trans-2-(4-tert-butylcyclohexyl)-1-iodoethane

Refernces