10-(2-methoxyethyl)-3-phenylbenzo[g]pteridine-2,4(3H,10H)-dione

Base Information

• Chemical Name: 10-(2-methoxyethyl)-3-phenylbenzo[g]pteridine-2,4(3H,10H)-dione
• CAS No.: 61369-43-5
• Molecular Formula: C19H16N4O3
• Molecular Weight: 348.361
• Mol file: 61369-43-5.mol

Synonyms:

Chemical Property of 10-(2-methoxyethyl)-3-phenylbenzo[g]pteridine-2,4(3H,10H)-dione

Chemical Property:

• Vapor Pressure: 1.8E-10mmHg at 25°C

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 10-(2-methoxyethyl)-3-phenylbenzo[g]pteridine-2,4(3H,10H)-dione

There total 8 articles about 10-(2-methoxyethyl)-3-phenylbenzo[g]pteridine-2,4(3H,10H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(methoxy-2-ethyl)-10-phenyl-3-tetrahydro-6,7,8,9-iso-alloxazine (61369-41-3) → (methoxy-2-ethyl)-10-phenyl-3-iso-alloxazine (61369-43-5)

Guidance literature:

palladium on activated charcoal; In decalin; for 1h; Heating;

Reference yield: 30.0%

amino-4(methoxy-2-ethyl)-10-phenyl-3-tetrahydro-6,7,8,10-benzopteridinone-2 (117286-28-9) → (methoxy-2-ethyl)-10-phenyl-3-iso-alloxazine (61369-43-5)

Guidance literature:

With triphenylmethyl alcohol; acide trifluoroacetique; for 12h; Heating;

Reference yield:

phenyl isocyanate (103-71-9) → (methoxy-2-ethyl)-10-phenyl-3-iso-alloxazine (61369-43-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 95 percent / CHCl₃ / 24 h / 20 °C

2: 90 percent / triethyl amine / methanol / 0.33 h / Heating

3: 30 percent / triphenylcarbinol, acide trifluoroacetique / 12 h / Heating

With triphenylmethyl alcohol; acide trifluoroacetique; triethylamine; In methanol; chloroform;

upstream raw materials:

(methoxy-2-ethyl)-10-phenyl-3-tetrahydro-6,7,8,9-iso-alloxazine

amino-4(methoxy-2-ethyl)-10-phenyl-3-tetrahydro-6,7,8,10-benzopteridinone-2

phenyl isocyanate

3-Amino-4-(2-methoxy-ethyl)-4,6,7,8-tetrahydro-quinoxaline-2-carbonitrile

Refernces