1H-Inden-1-ol, 2,3-dihydro-, 3,5-dinitrobenzoate

Base Information

• Chemical Name: 1H-Inden-1-ol, 2,3-dihydro-, 3,5-dinitrobenzoate
• CAS No.: 61463-15-8
• Molecular Formula: C16H12N2O6
• Molecular Weight: 328.281
• Mol file: 61463-15-8.mol

Synonyms:

Chemical Property of 1H-Inden-1-ol, 2,3-dihydro-, 3,5-dinitrobenzoate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Inden-1-ol, 2,3-dihydro-, 3,5-dinitrobenzoate

There total 2 articles about 1H-Inden-1-ol, 2,3-dihydro-, 3,5-dinitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

inden-1-one (83-33-0) → 3,5-dinitro-benzoic acid indan-1-yl ester (61463-15-8)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether

2: Py

With pyridine; lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1021/jo00428a037

Reference yield:

1-Indanol (6351-10-6) + 3,5-dinitrobenoyl chloride (99-33-2) → 3,5-dinitro-benzoic acid indan-1-yl ester (61463-15-8)

Guidance literature:

With pyridine;

DOI:10.1021/jo00428a037

Reference yield:

3,5-dinitro-benzoic acid indan-1-yl ester (61463-15-8) → 3,5-dinitrobenzoic acid (99-34-3) + 1-Indanol (6351-10-6)

Guidance literature:

With water; In acetone; at 60 ℃; Rate constant; Kinetics; Thermodynamic data; various temperatures; ΔH(excit.), ΔS(excit.);

DOI:10.1021/jo00341a027

upstream raw materials:

1-Indanol

3,5-dinitrobenoyl chloride

inden-1-one

Downstream raw materials:

3,5-dinitrobenzoic acid

1-Indanol