2-Propen-1-one, 3-(4-chlorophenyl)-1-phenyl-, oxime, (E,E)-

Base Information

• Chemical Name: 2-Propen-1-one, 3-(4-chlorophenyl)-1-phenyl-, oxime, (E,E)-
• CAS No.: 61571-80-0
• Molecular Formula: C15H12ClNO
• Molecular Weight: 257.719
• Mol file: 61571-80-0.mol

Synonyms:

Chemical Property of 2-Propen-1-one, 3-(4-chlorophenyl)-1-phenyl-, oxime, (E,E)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Propen-1-one, 3-(4-chlorophenyl)-1-phenyl-, oxime, (E,E)-

There total 3 articles about 2-Propen-1-one, 3-(4-chlorophenyl)-1-phenyl-, oxime, (E,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

4-chlorochalcone (24721-26-4,956-04-7,22252-16-0) → 3-(4-chlorophenyl)-1-phenylprop-2-en-1-one oxime (61571-80-0)

Guidance literature:

With potassium hydroxide; phosphate buffer; hydroxylamine hydrochloride; In ethanol; water; for 20h; Heating;

Reference yield:

4-chlorochalcone (24721-26-4,956-04-7,22252-16-0) → 3-(4-chlorophenyl)-1-phenylprop-2-en-1-one oxime (61571-80-0) + 3-(4-chlorophenyl)-1-phenylprop-2-en-1-one oxime (111149-62-3)

Guidance literature:

With pyridine; hydroxylamine hydrochloride; sodium sulfate; for 0.25h; Microwave irradiation;

DOI:10.2174/1570178614666170822163132

Reference yield:

→ 3-(4-chlorophenyl)-1-phenylprop-2-en-1-one oxime (61571-80-0)

Guidance literature:

3-(4-Chlorphenyl)-1-phenyl-propenon, NH2OH*HCl, A.;

DOI:10.1002/ardp.19763090912

upstream raw materials:

4-chlorochalcone

Downstream raw materials:

(E)-3-(4-chlorophenyl)-N-phenylacrylamide

Refernces

• 1、 Sinisterra, J. V.,Marinas, J. M.. "Ba(OH)2 AS THE CATALYST IN ORGANIC REACTIONS-PART X-REACTION OF CHALCONE WITH HYDROXYLAMINE". . p. 293 - 302. Retrieved 2007/10/02.