1,2,4,5-Tetrachloro-3,6-bis(dichloromethyl)benzene

Base Information

• Chemical Name: 1,2,4,5-Tetrachloro-3,6-bis(dichloromethyl)benzene
• CAS No.: 2142-31-6
• Molecular Formula: C8H2Cl8
• Molecular Weight: 381.7255
• European Community (EC) Number: 633-644-1
• DSSTox Substance ID: DTXSID60175687
• Nikkaji Number: J2.574.556F
• Wikidata: Q83046016
• Mol file: 2142-31-6.mol

Synonyms:2142-31-6;1,2,4,5-tetrachloro-3,6-bis(dichloromethyl)benzene;p-Xylene, alpha,alpha,alpha',alpha',2,3,5,6-octachloro-;Benzene, 1,2,4,5-tetrachloro-3,6-bis(dichloromethyl)-;1,4-bis(dichloromethyl)-2,3,5,6-tetrachlorobenzene;SCHEMBL6820133;DTXSID60175687;AKOS004905103;p-Xylene, .alpha.,.alpha.,.alpha.',.alpha.',2,3,5,6-octachloro-,

Chemical Property of 1,2,4,5-Tetrachloro-3,6-bis(dichloromethyl)benzene

Chemical Property:

• Boiling Point: 377.5°Cat760mmHg
• Flash Point: 181.5°C
• PSA: 0.00000
• Density: 1.759g/cm³
• LogP: 7.25260
• XLogP3: 6.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 381.760571
• Heavy Atom Count: 16
• Complexity: 192

Purity/Quality:

99% ^*data from raw suppliers

ALPHA,ALPHA,ALPHA',ALPHA'-2,3,5,6-OCTACHLORO-P-XYLENE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1(=C(C(=C(C(=C1Cl)Cl)C(Cl)Cl)Cl)Cl)C(Cl)Cl

Technology Process of 1,2,4,5-Tetrachloro-3,6-bis(dichloromethyl)benzene

There total 4 articles about 1,2,4,5-Tetrachloro-3,6-bis(dichloromethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,2,4,5-tetrachlorobenzene (95-94-3) + chloroform (67-66-3,8013-54-5) → 1,4-bis(dichloromethyl)-2,3,5,6-tetrachlorobenzene (2142-31-6)

Guidance literature:

aluminium trichloride; for 22h; Heating;

DOI:10.1021/jo00018a046

Reference yield:

→ 1,4-bis(dichloromethyl)-2,3,5,6-tetrachlorobenzene (2142-31-6)

Guidance literature:

at 120 ℃; beim Chlorieren im Licht;

Reference yield:

1,2,4,5-tetrachloro-3,6-dimethyl-benzene (877-10-1) → 1,4-bis(dichloromethyl)-2,3,5,6-tetrachlorobenzene (2142-31-6)

Guidance literature:

With tetrachloromethane; chlorine; Irradiation;

upstream raw materials:

1,2,4,5-tetrachloro-3,6-dimethyl-benzene

1,2,4,5-tetrachlorobenzene

chloroform

Downstream raw materials:

αH,α'H-tetraicosachloro-α,α,α',α'-tetraphenyl-p-xylene

perchloro-α,α,α',α'-tetraphenyl-p-xylylene

1,4-bis(difluoromethyl)-2,3,5,6-tetrafluorobenzene

2,3,5,6-tetrachlorobenzene-1,4-dicarbonitrile oxide

Refernces

• 1、 Dolbier Jr., William R.,Xie, Puhui,Zhang, Lianhao,Xu, Wei,Chang, Ying,Abboud, Khalil A.. "Synthesis of perfluoro[2.2]paracyclophane". . p. 2469 - 2472. Retrieved 2008/09/19.
• 2、 Castaner, J.,Riera, J.. "Highly Crowded Perchloropolyphenyl-p-xylylenes with Exceptional Thermal Stability". . p. 5445 - 5448. Retrieved 2007/10/02.