Hexane-2,3-diol

Base Information

• Chemical Name: Hexane-2,3-diol
• CAS No.: 617-30-1
• Molecular Formula: C6H14O2
• Molecular Weight: 118.176
• Mol file: 617-30-1.mol

Synonyms:2,3-Hexanediol;Hexan-2,3-diol;RS-2,3-hexanediol;

Chemical Property of Hexane-2,3-diol

Chemical Property:

• Melting Point: 60°C
• Refractive Index: 1.4510
• Boiling Point: 221.7°C (rough estimate)
• PSA: 40.46000
• Density: 0.9900
• LogP: 0.52820

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hexane-2,3-diol

There total 2 articles about Hexane-2,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-hexene (592-41-6,25067-06-5) → n-hexan-2-ol (626-93-7) + 1-hexene-3-ol (4798-44-1,67928-93-2) + 2,3-hexanediol (617-30-1) + hexane-3,4-diol (922-17-8)

Guidance literature:

1-hexene; at 25 ℃; for 40h; Irradiation;

With water; In acetonitrile;

Reference yield:

2-hexene (592-43-8) → 2-methylpent-1-en-3-ol (96481-55-9,2088-07-5) + hex-3-en-2-one (763-93-9) + 2,3-hexanediol (617-30-1) + hexane-3,4-diol (922-17-8) + 4-hexen-3-one (2497-21-4,50396-87-7,50396-96-8,130981-55-4,25659-22-7) + 4-hexen-3-ol

Guidance literature:

2-hexene; at 25 ℃; for 14h; Irradiation;

With water;

Reference yield: 70.0%

2,3-hexanediol (617-30-1) → 2,5-dimethyltetrahydrofuran (1003-38-9)

Guidance literature:

With N-heterocyclic carbene-iridium(III) complex; In toluene; tert-butyl alcohol; for 24h; Inert atmosphere; Reflux;

DOI:10.1002/chem.201805460

upstream raw materials:

1-hexene

2-hexene

Downstream raw materials:

carbon dioxide

acetic acid

butyric acid

2,5-dimethyltetrahydrofuran

Refernces