1-Chloroindan

Base Information

• Chemical Name: 1-Chloroindan
• CAS No.: 35275-62-8
• Molecular Formula: C9H9Cl
• Molecular Weight: 152.623
• Hs Code.: 2903999090
• European Community (EC) Number: 252-480-8
• DSSTox Substance ID: DTXSID00956715
• Nikkaji Number: J100.047K
• Mol file: 35275-62-8.mol

Synonyms:1-chloro-2,3-dihydro-1H-indene;1-Chloroindan;35275-62-8;1-Chloroindane;EINECS 252-480-8;1H-Indene, 1-chloro-2,3-dihydro-;.alpha.-Chlorindane;indanyl chloride;alpha-Chlorindane;1-Chloroindane #;Indane, 1-chloro-;SCHEMBL1117278;DTXSID00956715;AMY39231;MFCD09608063;AKOS009235584;AC-3552;BS-53246;CS-0155923;FT-0651938;E76732;EN300-186764;A822707

Chemical Property of 1-Chloroindan

Chemical Property:

• Vapor Pressure: 0.11mmHg at 25°C
• Refractive Index: 1.57
• Boiling Point: 228.5 °C at 760 mmHg
• Flash Point: 76.2 °C
• PSA: 0.00000
• Density: 1.15 g/cm³
• LogP: 2.91270
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 152.0392780
• Heavy Atom Count: 10
• Complexity: 122

Purity/Quality:

99% ^*data from raw suppliers

1-chloro-2,3-dihydro-1H-indene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC2=CC=CC=C2C1Cl

Technology Process of 1-Chloroindan

There total 9 articles about 1-Chloroindan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-Indanol (6351-10-6) → 1-chloroindane (35275-62-8)

Guidance literature:

With thionyl chloride; In toluene; at 55 ℃; for 1h;

DOI:10.1021/jm950759z

Reference yield: 6.0%

1-Indanol (6351-10-6) → 1-chloroindane (35275-62-8) + 1-indene (95-13-6)

Guidance literature:

With pyridine; bis(trichloromethyl) carbonate; In tetrahydrofuran; Ambient temperature;

DOI:10.1021/jo00025a046

Reference yield:

1-indene (95-13-6) → 1-chloroindane (35275-62-8)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

1-Indanol

1-indene

hydrogenchloride

inden-1-one

Downstream raw materials:

indan-1-yl-o-tolyl-amine

Indan-1-carboxylic acid

1-cyanoindane

Refernces

• 1、 Ajvazi, Njomza,Stavber, Stojan. "Direct halogenation of alcohols with halosilanes under catalyst- and organic solvent-free reaction conditions". supporting information. p. 2430 - 2433. Retrieved 2016/05/19.
• 2、 Chen, Ying-Zhe,Ni, Ching-Wen,Teng, Fu-Lin,Ding, Yi-Shun,Lee, Tunng-Hsien,Ho, Jinn-Hsuan. "Construction of polyaromatics via photocyclization of 2-(fur-3-yl) ethenylarenes, using a 3-furyl group as an isopropenyl equivalent synthon". . p. 1748 - 1762. Retrieved 2014/03/21.