1,1,3-tribromopropane

Base Information

• Chemical Name: 1,1,3-tribromopropane
• CAS No.: 23511-78-6
• Molecular Formula: C3H5 Br3
• Molecular Weight: 280.785
• Mol file: 23511-78-6.mol

Synonyms:1,1,3-Tribromopropane

Chemical Property of 1,1,3-tribromopropane

Chemical Property:

• Vapor Pressure: 0.193mmHg at 25°C
• Boiling Point: 217.7°Cat760mmHg
• Flash Point: 86.1°C
• Density: 2.379g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,1,3-tribromopropane

There total 6 articles about 1,1,3-tribromopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethene (74-85-1) + Bromoform (75-25-2) → 1,1,3-trichloropropane (23511-78-6)

Guidance literature:

With dibenzoyl peroxide;

Reference yield:

Bromoform (75-25-2) + acrylonitrile (107-13-1,25014-41-9) → 1,1,3-trichloropropane (23511-78-6) + 2,4,4-Tribromo-butyronitrile (111398-11-9)

Guidance literature:

With iron pentacarbonyl; N,N-dimethyl-formamide; at 95 - 100 ℃; for 2h; Yields of byproduct given;

DOI:10.1007/BF00960160

Reference yield:

acrolein (107-02-8,25068-14-8) → 1,1,3-trichloropropane (23511-78-6)

Guidance literature:

With hydrogen bromide; dann mit PBr₂Cl₃;

upstream raw materials:

ethene

Bromoform

acrolein

1-chloro-1,3-dibromopropane

Downstream raw materials:

cyclopropyl bromide

cyclopropyliodide

Refernces

• 1、 Vasil'eva, T. T.,Velichko, F. K.,Kochetkova, V. A.,Bondarenko, O. P.. "REACTION OF BROMOFORM AND IODOFORM WITH ACRYLIC MONOMERS INITIATED BY Fe(CO)5 + DMF". . p. 1765 - 1768. Retrieved 2007/10/02.