Selenium diimide, bis(phenylsulfonyl)-

Base Information

• Chemical Name: Selenium diimide, bis(phenylsulfonyl)-
• CAS No.: 61945-92-4
• Molecular Formula: C12H10N2O4S2Se
• Molecular Weight: 389.314
• Mol file: 61945-92-4.mol

Synonyms:

Chemical Property of Selenium diimide, bis(phenylsulfonyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Selenium diimide, bis(phenylsulfonyl)-

There total 5 articles about Selenium diimide, bis(phenylsulfonyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

difluoro-N-phenylsulfonylselenimide (83215-02-5) → N,N'-di(phenylsulfonyl)selenium diimide (61945-92-4)

Guidance literature:

With Hexamethyldisiloxane; In 1,2-dichloro-ethane; at 20 ℃; for 1h;

Reference yield: 70.0%

N,N-bis(trimethylsilyl)benzenesulfonamide (1023-95-6) → Hexamethyldisiloxane (107-46-0) + N,N'-di(phenylsulfonyl)selenium diimide (61945-92-4)

Guidance literature:

With selenyl fluoride; In 1,2-dichloro-ethane; at 20 ℃; for 1h;

Reference yield:

N,N-bis(trimethylsilyl)benzenesulfonamide (1023-95-6) → N,N'-di(phenylsulfonyl)selenium diimide (61945-92-4)

Guidance literature:

With selenium(IV) fluoride; In diethyl ether;

upstream raw materials:

N,N-bis(trimethylsilyl)benzenesulfonamide

difluoro-N-phenylsulfonylselenimide

C₆H₁₈N₂SeSi₂

benzenesulfonyl chloride

Downstream raw materials:

N,N-Dichlorobenzenesulfonamide

1-(phenylsulfonylamino)-9-(phenylsulfonylimino)-9-selenoperhydrofluorene

N-phenylsulfonyl-Se,Se-diphenylselenimide

N-benzylidenephenylsulfonamide

Refernces

• 1、 Derkach, N. Ya.,Barashenkov, G. G.,Levchenko, E. S.. "N,N'-DIACYLSELENIUM DIIMIDES III. NEW METHODS OF SYNTHESIS". . p. 837 - 839. Retrieved 2007/10/02.