Butanoic acid, 2-amino-, monopotassium salt

Base Information

• Chemical Name: Butanoic acid, 2-amino-, monopotassium salt
• CAS No.: 62123-45-9
• Molecular Formula: C₄H₈NO₂*K
• Molecular Weight: 141.211
• Mol file: 62123-45-9.mol

Synonyms:

Chemical Property of Butanoic acid, 2-amino-, monopotassium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Butanoic acid, 2-amino-, monopotassium salt

There total 1 articles about Butanoic acid, 2-amino-, monopotassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-aminobutanol (96-20-8,13054-87-0) → potassium α-aminobutyrate (62123-45-9)

Guidance literature:

With (6-di-tert-butylphosphinomethyl-2,2’-bipyridyl)Ru(CO)HCl; water; potassium hydroxide; In 1,4-dioxane; for 24h; Schlenk technique; Inert atmosphere; Glovebox; Reflux;

DOI:10.1021/jacs.6b03488

Reference yield: 95.0%

(2-methyl-4-oxopent-2-yl)diphenylphosphine oxide (35078-70-7) + potassium α-aminobutyrate (62123-45-9) → potassium 2-[4-methyl-4-(diphenylphosphoryl)pent-2-ylideneamino]butyrate

Guidance literature:

In methanol; for 4h; Reflux;

DOI:10.1134/S1070363217040363

Reference yield: 37.0%

4-nitrophenylhydrazone of (diisopropoxyphosphoryl)formyl chloride (123434-39-9) + potassium α-aminobutyrate (62123-45-9) → 2-(diisopropoxyphosphoryl)-2-(4-nitrophenylazo)-4-ethyloxazolidin-5-one (132122-87-3)

Guidance literature:

In isopropyl alcohol; at 20 - 25 ℃; for 168h;

upstream raw materials:

2-aminobutanol

Downstream raw materials:

2-(diisopropoxyphosphoryl)-2-(4-nitrophenylazo)-4-ethyloxazolidin-5-one

Refernces

• 1、 Hu, Peng,Ben-David, Yehoshoa,Milstein, David. "General Synthesis of Amino Acid Salts from Amino Alcohols and Basic Water Liberating H2". supporting information. p. 6143 - 6146. Retrieved 2016/06/09.