1,4,6-Triphenyl-2-pyridone

Base Information

• Chemical Name: 1,4,6-Triphenyl-2-pyridone
• CAS No.: 62257-63-0
• Molecular Formula: C23H17NO
• Molecular Weight: 323.38700
• Hs Code.: 2933399090
• Mol file: 62257-63-0.mol

Synonyms:2(1H)-Pyridinone,1,4,6-triphenyl;N,4,6-Triphenyl-2-pyridon;1,4,6-triphenyl-1H-pyridin-2-one;1,4,6-Triphenyl-2-pyridone;1,4,6-Triphenyl-2(1H)-pyridinone;

Chemical Property of 1,4,6-Triphenyl-2-pyridone

Chemical Property:

• PSA: 22.00000
• LogP: 5.17150

Purity/Quality:

99%min ^*data from raw suppliers

1,4,6-TRIPHENYL-2-PYRIDONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4,6-Triphenyl-2-pyridone

There total 6 articles about 1,4,6-Triphenyl-2-pyridone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Acetanilid (103-84-4) + 1,3-diphenyl-2-propynone (7338-94-5) → 1,4,6-triphenyl-2(1H)-pyridinone (62257-63-0)

Guidance literature:

With potassium hydroxide; In 1,4-dioxane; at 100 ℃; for 6h; Sealed tube; Green chemistry;

DOI:10.1039/c8gc00069g

Reference yield: 77.0%

N-(4,6-diphenyl-2H-pyran-2-ylidene)benzeneamine (55263-05-3) → 1,4,6-triphenyl-2(1H)-pyridinone (62257-63-0)

Guidance literature:

With sodium methylate; In methanol; for 24h; Heating;

DOI:10.1016/S0040-4020(99)00958-8

Reference yield: 65.0%

2-methyl-1,4,6-triphenylpyridinium tetrafluoroborate → 1,4,6-triphenyl-2(1H)-pyridinone (62257-63-0)

Guidance literature:

With n-Amyl nitrite; sodium ethanolate; In ethanol; at 5 ℃; for 15h;

upstream raw materials:

N-(4,6-diphenyl-2H-pyran-2-ylidene)benzeneamine

aniline

Acetanilid

1,3-diphenyl-2-propynone

Refernces

• 1、 Uncuta, Cornelia,Tudose, Adriana,Caproiu, Miron Teodor,Plaveti, Marieta,Kakou-Yao, Rita. "Beckmann and cyclization reactions of δ-oxo-α,β- unsaturated ketoximes obtained from pyrylium salts and hydroxylamine. Formation of 2-aryl(or alkyl)amino-4,6- disubstituted pyrylium salts". . p. 15011 - 15024. Retrieved 2007/10/03.