2-Prop-2-enoxycarbonyloxyethyl prop-2-enyl carbonate

Base Information

• Chemical Name: 2-Prop-2-enoxycarbonyloxyethyl prop-2-enyl carbonate
• CAS No.: 4074-91-3
• Molecular Formula: C10H14 O6
• Molecular Weight: 230.218
• NSC Number: 32642,19169
• DSSTox Substance ID: DTXSID70280953
• Nikkaji Number: J2.076.670K
• Wikidata: Q82014651
• Mol file: 4074-91-3.mol

Synonyms:4074-91-3;2-prop-2-enoxycarbonyloxyethyl prop-2-enyl carbonate;NSC19169;SCHEMBL176184;DTXSID70280953;NSC32642;NSC 19169;NSC 32642;NSC-19169;NSC-32642;Bis(carbonic acid allyl)ethylene ester

Chemical Property of 2-Prop-2-enoxycarbonyloxyethyl prop-2-enyl carbonate

Chemical Property:

• Vapor Pressure: 0.00577mmHg at 25°C
• Boiling Point: 273.3°C at 760 mmHg
• Flash Point: 114.3°C
• Density: 1.131g/cm³
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 11
• Exact Mass: 230.07903816
• Heavy Atom Count: 16
• Complexity: 222

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCOC(=O)OCCOC(=O)OCC=C

Technology Process of 2-Prop-2-enoxycarbonyloxyethyl prop-2-enyl carbonate

There total 4 articles about 2-Prop-2-enoxycarbonyloxyethyl prop-2-enyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diallylcarbonate (15022-08-9) + ethylene glycol (107-21-1) → [1,3]-dioxolan-2-one (96-49-1) + 2,5-dioxa-adipic acid diallyl ester (4074-91-3) + 2-propenyl-2'-hydroxyethyl carbonate

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 24h; Inert atmosphere;

DOI:10.1002/chem.201103418

Reference yield:

diallylcarbonate (15022-08-9) + ethylene glycol (107-21-1) → 2,5-dioxa-adipic acid diallyl ester (4074-91-3) + 2-propenyl-2'-hydroxyethyl carbonate

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine; In dimethyl sulfoxide; at 20 - 25 ℃; for 24h; Inert atmosphere;

DOI:10.1002/chem.201103418

Reference yield:

ethylenebis(chloroformate) (124-05-0) + allyl alcohol (107-18-6) → 2,5-dioxa-adipic acid diallyl ester (4074-91-3)

Guidance literature:

With sodium hydroxide; at 0 - 5 ℃;

upstream raw materials:

ethylene glycol

Allyl chloroformate

ethylenebis(chloroformate)

allyl alcohol

Refernces