Technology Process of Benzenemethanol, a-[(3E)-4-phenyl-3-butenyl]-
There total 9 articles about Benzenemethanol, a-[(3E)-4-phenyl-3-butenyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
cinnamylideneacetophenone;
With
indium(III) chloride; sodium tetrahydroborate;
In
acetonitrile;
at 28 - 30 ℃;
for 2h;
With
methanol;
In
acetonitrile;
DOI:10.1016/j.tet.2003.08.022
- Guidance literature:
-
(Z)-cinnamyl alcohol;
With
silver hexafluoroantimonate; tetrakis(actonitrile)copper(I) hexafluorophosphate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 4-nitro-benzoic acid;
In
1,4-dioxane; water; acetonitrile;
at 20 ℃;
for 0.166667h;
Schlenk technique;
styrene;
In
1,4-dioxane; water; acetonitrile;
at 100 ℃;
for 23h;
regioselective reaction;
Schlenk technique;
DOI:10.1002/anie.201813148
- Guidance literature:
-
(2E)-3-phenyl-2-propen-1-ol;
With
silver hexafluoroantimonate; water; 1,4-di(diphenylphosphino)-butane; acetonitrile; copper(l) chloride; 4-nitro-benzoic acid;
In
tetrahydrofuran;
at 20 ℃;
for 0.166667h;
Inert atmosphere;
styrene;
In
tetrahydrofuran;
at 100 ℃;
for 23h;
Inert atmosphere;
