Glyoxal mono-dimethylhydrazone

Base Information

• Chemical Name: Glyoxal mono-dimethylhydrazone
• CAS No.: 62506-63-2
• Molecular Formula: C4H8N2O
• Molecular Weight: 100.12
• Hs Code.: 2928000090
• European Community (EC) Number: 625-059-5
• DSSTox Substance ID: DTXSID90446291
• Mol file: 62506-63-2.mol

Synonyms:Glyoxal mono-dimethylhydrazone;62506-63-2;(2E)-2-(dimethylhydrazinylidene)acetaldehyde;2-(2,2-Dimethylhydrazineylidene)acetaldehyde;133643-19-3;SCHEMBL13250396;DTXSID90446291;Glyoxal mono-dimethylhydrazone, 97%;(E)-2-(2,2-Dimethylhydrazono)acetaldehyde

Chemical Property of Glyoxal mono-dimethylhydrazone

Chemical Property:

• Boiling Point: 90 °C(Press: 16 Torr)
• PKA: -0.77±0.70(Predicted)
• PSA: 32.67000
• Density: 0.93±0.1 g/cm3(Predicted)
• LogP: -0.26730
• Storage Temp.: 2-8°C
• XLogP3: 0.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 100.063662883
• Heavy Atom Count: 7
• Complexity: 77.8

Purity/Quality:

98%Min ^*data from raw suppliers

GLYOXAL MONO-DIMETHYLHYDRAZONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): 1922146
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CN(C)N=CC=O
• Isomeric SMILES: CN(C)/N=C/C=O

Technology Process of Glyoxal mono-dimethylhydrazone

There total 2 articles about Glyoxal mono-dimethylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Glyoxal (131543-46-9,107-22-2) + N,N-Dimethylhydrazine (57-14-7) → glyoxal mono(dimethylhydrazone) (62506-63-2)

Guidance literature:

In water;

Reference yield:

→ glyoxal mono(dimethylhydrazone) (62506-63-2)

Guidance literature:

Reference yield: 89.0%

glyoxal mono(dimethylhydrazone) (62506-63-2) + methylmagnesium bromide (75-16-1) → 2-hydroxypropanal N,N-dimethylhydrazone (222302-26-3)

Guidance literature:

In tetrahydrofuran; at -40 ℃;

DOI:10.1016/S0040-4020(98)01087-4

upstream raw materials:

Glyoxal

N,N-Dimethylhydrazine

Downstream raw materials:

4-<2-(Dimethylhydrazono)ethyliden>-2-phenyl-2-oxazolin-5-on

2-<(Dimethylhydrazono)ethyliden>cyclohexanon

4-Dimethylhydrazono-1-(4-methoxyphenyl)-2-buten-1-on

4-Dimethylhydrazono-2-methoxyphenyl-2-buten-1-on

Refernces

• 1、 -. "Compositions of retinoids substituted with a dithiane ring, their use, and process for preparing the compounds". . . Retrieved 2008/06/13.
• 2、 -. "Anti-inflammatory 4,5-diaryl-α-(polyfluoroalkyl)-1H-pyrrole-2-methanamines". . . Retrieved 2008/06/13.