Technology Process of 6-(Methylsulfanyl)hexan-1-amine
There total 19 articles about 6-(Methylsulfanyl)hexan-1-amine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
diethyl ether;
for 0.333333h;
Ambient temperature;
DOI:10.1007/BF00598411
- Guidance literature:
-
With
hydrogenchloride;
In
benzene;
at 80 ℃;
for 1h;
DOI:10.1007/BF00597577
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 65 percent / PBr3 / pyridine; diethyl ether / 1.) -30 deg C, 3h, 2.) 12h, 25 deg C
2: 56 percent / sodium azide / 2-ethoxy-ethanol; H2O / 24 h / 90 °C
3: 95 percent / lithium tetrahydroaluminate / diethyl ether / 0.33 h / Ambient temperature
With
lithium aluminium tetrahydride; sodium azide; phosphorus tribromide;
In
pyridine; 2-ethoxy-ethanol; diethyl ether; water;
DOI:10.1007/BF00598411
